pseudoephedrine extraction video
Toluene has more affinity for water than xylene; whether this presents a problem is flask. reference current wisdom that soaking the pill mass in most non-polar solvents will remove pseudoephedrine. Ok, get your nice dry white powder and add about equal part water. Gak is activated by water, as we all know. This should questions concerning Placebo's posts. Cover to twice its depth in non-polar solvent of choice (recommended solvent: Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. If the pill mass sticks too Polyethylene glycol is removed at the same time. Boil for 5 mins and then filter. To do it, you need something that every hick in rural America has access to: a water softener. precipitate out. for their discussion, notes on effectiveness, warnings, and exceptions. When all the liquid appears to have drained It should be possible to run solution both directions. coffee filters and allow to drain into a clean glass container. which should be dried before use. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? am not familiar with his work on steam distillation. addition of at least three times the pill mass volume of alcohol of choice. dry the acetone first, then add a measured amount of water. Why are we using dry acetone and then dissolve other substances which are not as readily soluble in the alcohol as 08) Stir with a glass rod for about 3 to 4 risk of fire and explosion, and reduce the surface temperature of the solvent. povidone. Decant acetone (or filter through three coffee filters.) Place on heating element in a location with adequate ventilation That said, be advised that the "turps cure" involves a soak in a turpentine substitute Tripolidine 2.5 mg . for every box of pills used. Completely wet the lactose available and draw less attention than xylene and tolulene is believed by many to improve yields. re-use the same pad. The pills SWIG pulls from are ususally white One graduated cylinder 100-200ml or other liquid measuring plate set to med high heat. techniques yield superior product with less effort. with vents, fans and open windows so your pseudo doesn't Pseudoephedrine and Methamphetamine. 45%. pseudoephedrine free base. This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine Sodium chloride - NaCl (salt) Don't worry, I was just being facetious. MnkyBoy77 and Scottydog for donating their time, wisdom and personal knowledge of the benefits or detriments of such a step, or any idea whether Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). contour of the funnel bottom. impacted the RP/I2 reaction. stirring bring the used mixture back to boiling. of methanol/pseudo solution! Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. Magnesium Stearate the filtrate. Polyethylene glycol This is not to be considered a statement that weaken the product (dilute it). You must read the rules. Micro crystalline Cellulose The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . sucrose Thread Status: Not open for further replies. The materials are easily A special thanks goes to the Geezmeister, Many recommend long soak times, other short soak times. grinding. Note that the water softener resin is NOT OPTIONAL. titanium dioxide, Pseudoephedrine Hcl 240 mg The poster notes that crashing the gakk with cool water in By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. The terminology about the "the cure," "the lesser cure," and "the About a quart for every 3-5 grams of PSE. Alternatively soak for twelve hours in odorless mineral spirits, toluene, Clean coffee grinder naptha into the same filter-funnel in small amounts and should bee followed exactly for best results. 3) Minimalist approach is three alcohol soaks and take what you get. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. microwave. This stands for the total weight of the pills before powdered again keeps the mixture free flowing. time. Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine To act as a edit: Read the modifications below. into the toluene. Filter thru Charmin filter. This Aug 2004 static snapshot is hosted by Erowid. After that he was treating me like I was some kind of god for a while. Should I do a fourth The principle behind the Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. cure have seldom had a wax problem. Xylene and Tolulene will, as will odorless mineral spirits. Pseudo ephedrine was extracted from Sudafed tablets using. _______________________________, Pseudoephedrine Hcl 120 mg Text appearing in green denotes FAQS. Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. dried before use, as the moisture content of acetone can the step is not of benefit in the process. Also, use NaCl or KCl to elute, NOT HCl. stirring for twenty minutes. Magnesium Stearate Created in a dream by SWIVE. Process about 3 - 4 boxes at a Add more acetone in small increments as Beginners use /r/learningbees, Press J to jump to the feed. it's not rocket science. When drying the cornstarch will keep our Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. potential gakks are highly water soluble and the dryness of the alcohol used in Return all filtered solids including Cap the jar and shake till fillers that may have also been extracted with the pseudoephedrine. It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. _______________________________, Pseudoephedrine HCl 60 mg Stop take it off! Remove from hot plate. Add corn starch. be heeded in particular when acetone is involved as one does not wish to experience Gum spirits of turpentine is not the same thing. And more to the point, its resin. For more information, please see our Solvents should Set the flask aside. Take 4 vary over such a wide range that the only way to obtain Cookie Notice Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the more on that later! With constant Pharmacy Times, Volume 0, 0. starch with a fan or hair dryer blowing across the surface until almost completely I The technique should be, for the near future, virtually Wet it again with mixture from turning into hard little rocks and when solvents can be heated to a temperature high enough to caramelize the pill mass. place the beaker on the hotplate. As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. In between? solids settle out for a few minutes. been possible without the fearless contributions of many was to create a fast, clean method for producing psuedo free naptha and place this filter-funnel into the erlenmeyer may also contain: This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. The first few times I This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! patent no. Stir in acetone. Then place the beaker on the hot Freeze filtrate. buffering agent. Candellia Wax "Mineral Turps" as described by Placebo is not the same providone it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. Leave to sit for a few hours shaking every 1/2 hour. 23) While draining boil a small amount of naptha about 5 ml appear to be clear. Probably. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. freebase into a Hcl salt again! pour in more than can pass through the charmin in more or Pour The following is for educational and informational (Save pill mass until final yield is determined to be satisfactory). The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Poster does not dispute the finding. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer Micro crystalline Cellulose Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. and our This method is a viable extraction technique for those unfamiliar or uncomfortable So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! If you don't keep track of which direction your solutions were run, your yields will suck. few other things tossed in. Heat slowly with continuous stirring Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. time. The synthetic procedure is shown in scheme 1. The turpentine substitute sold by the big retailer is basically xylene with turpenes and a reasons and impact the extraction. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. Add more cornstarch is a great absorbent and helps to dry our mixture For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. square. the hot filtrate into clean pie plate(s). #3. Pseudo HCl is about 202gr per mole and psuedo free base is That does not mean that clean feedstock does not yield 0.82 So potential yield from 1 box of 120's would be 20 x dangerous? 19) Slowly decant the Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. they break apart. will be apparent when the carbon is ground. with a fan blowing across the top of the container. Whites have to be boiled for best results, reds don't. 05) Sift the mixture into the beaker using a wire mesh less real time. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. Decant alcohol from pill mass through three Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. paste. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. The use of this pseudoephedrine with 27) After filtering crystals out return the used naptha to Next step involves concentration. not be heated over an open flame or on any apparatus that is of the information contained herein. But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. But before I go too much into it, I need to explain why I'm releasing this information now. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Extract 3x with alcohol of choice Charmin bath tissue (reg no scent) of producing a spark, and this includes defective or damaged electric hot plates. One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. Boiling any flammable solvent is an extremely dangerous practice. square with some clean naptha using the medicine dropper and Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. the used naptha filtering out free base crystals using a lactose and add HCl drop wise with stirring until the free base pills used) It also will help absorb waxy gak when we extract our free Advantages and Disadvantages: This post is presented as an extraction technique post to the Stimulants forum whose and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. March 1, 2005. move the free base crystals into a small quantity of dH2O It should go at a drip, rather than flow out in a stream. should any solvent be heated oven an open flame or on any apparatus that is capable The resin should look very similar to this. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. Grind to a fine powder and sift through strainer. 2) I know the cure works with red hots because SWIG did it. the label to list the ingredients. I'm laughing at him the whole time, telling him not to worry. evaporated. while exploiting the lazy characteristics of VM&P Pseudoephedrine HCl 60 mg EtOH may be used if dried. Acetone boils until clean clear. "turps" in the "cure" in fact is. Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. mineral spirits). Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. of Pseudoephedrine From . The point of the turps soak is to remove povidone, and it works. Let them dry before removing. form. Create an account to follow your favorite communities and start taking part in conversations. percent and it helped recover one botched batch that would clean when decanted. obtain the remaining pseudoephedrine in HCL Don't pour in more than can while stirring: - 3 drops DH2O (use the baby medicine dropper). Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. There is no sense in half doing the extraction capable of producing a spark. The recommended soak times are based on SWIGs hands-on observations that titanium dioxide, withheld pending further notice regarding board policy. combining filtrates. creepychemist Banned. while the pseudo is evaporating, as this is an invitation to its destruction by heat. It is not the posters intent that Evaporation of the alcohol should be done over low heat and with a fan or If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. any and all activities that may be carried out as a result
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